3CAHC1 | Methodes chromatographiques | Materials and Chemistry | S9 | ||||||
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Lessons : 15 h | TD : 0 h | TP : 0 h | Project : 0 h | Total : 15 h | |||||
Co-ordinator : Pascal Cardinael |
Prerequisite | |
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Fundamental quantities in chromatography The basics of GC and CPG Works: -Chemical analysis methods and instrumental techniques, Francis Rouessac, Annick Rouessac, Daniel Cruché, et al., Collection: Sciences Sup, Dunod 2009-7th edition -Analytical chemistry, Douglas A. Skoog, Stanley R. Crouch, F. James Holler, Donald M. West Translation: Claudine Buess-Herman, Josette Danner 2012 Editor: De Boeck |
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Course Objectives | |
Acquire the necessary tools to develop the analysis of all types of organic compounds in HPLC and introduce students to the latest innovations in separative methods | |
Syllabus | |
1-Optimization of the analysis 2 – Analysis of polar and ionizable compounds (choice of stationary phase, mobile phase...) 3 – High temperature liquid chromatography (HTLC) and ultra high pressure chromatography (U-HPLC) practical advantages and constraints 4-Theoretical and practical Aspects of miniaturization 5 – Detection and coupling 6 – Analysis of chiral compounds by GC and HPLC 7 – Two-dimensional and multidimensional chromatography |
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Practical work (TD or TP) | |
Non renseigné | |
Acquired skills | |
-Control of the development of an analysis in HPLC including the choice of the column and the operating parameters. -Control of multidimensional gas chromatography methods. |
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Bibliography | |
- Chromatographies en phases liquide et super critique Rosset R., Caude M. et Jardy A. 1996 - 3è éd., Masson - Introduction to modern liquid chromatography (3rd Ed.)Auteurs : Snyder Lloyd R., Kirkland Joseph J., Dolan John W.Wiley 2010 - Chromatographic enantioseparation: Methods and applications, S. G. Allenmark. (1988). Ellis Horwood, Chichester |
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